The present invention belongs to a preparation method of fibre active carbon. Said invention uses viscose fibre as raw material, uses mixed phosphate and water vapour as activating agent and adopts a combined activating mode of carbonizing, chemical and physical process to obtain the invented fibre active carbon with high yield, tensile-strength and softness. The specific surface area of said product can be regulated in 1000 m2/g-2000m2/g by changing technological conditions, and its product yield is between 12-36 wt%. |