Original document(7 pages) Authorized document(7 pages) 中文版
    The method for preparing acetaminophen relates to a technological process for making hydrogenation reduction of p-nitrophenol and acetylation reaction of p-aminophenol in same process and adopting acetic acid and acid anhydride to make combined acidation. Said invention is characterized by that in medium acetic acid/acetic acid aqueous solution, under the action of catalyst the p-nitrophenol can be reduced into p-aminophenol by means of catalytic hydrogenation, then the catalyst is filtered from reduction product, said product can be acidated by using acetic acid in the medium at 100-150 deg.C, the conversion rate of p-aminophenol is 30-80%, then the excess acetic anhydride can be added at 50-100 deg.c to make p-aminophenol completely acidate, then the above-mentioned is separated and refined so as to obtain the acetaminophen finished product.
Application Number
申请号
03112820 Application Date
申请日
2003.02.11
Title 名称 Process for prepraring p-acetpamidophenol
Publication Number
公开号
1434026 Publication Date
公开日
2003.08.06
Approval Pub. Date Granted Pub. Date 2005.03.23
International Classification 分类号 C07C233/26,C07C231/10,C07C209/36
Applicant(s) Name
申请人
Nanjing Chemical Plant, SINOPEC
Address 地址 210038
Inventor(s) Name 发明人 Dai Jie, Luo Yongjun
Attorney & Agent 代理人 shen lian

  
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