The invention relates to a method used to leach separating metal especial cobalt and copper from copper cobalt iron alloy. It includes the following steps: melting the alloy at 1300-1550 degree centigrade; atomizing to alloy powder by high pressure air or water vapor; mixing the alloy powder with flux to process heat treatment; using mineral acid to dissolve the cobalt and iron but remain the copper after smashing; or directly using the mineral acid while adding oxidizing agent into the atomized alloy powder. It has the advantages of simple, high leaching efficiency. And it is fit for industrialization production. |