The present invention discloses process of compounding bright nickel plating solution with several kinds of organic additive for permanent magnetic Nd-Fe-B material. The organic additives include at least brightening agent and wetting agent, and the brightening agent includes primary brightening agent and secondary brightening agent. The process of compounding bright nickel plating solution includes the following steps: compounding blank electroplating solution without brightening agent, optimizing the type and concentration of secondary brightening agent and wetting agent while maintaining primary brightening agent, optimizing the type and concentration of primary brightening agent, and real-time regulating additive concentration to ensure stable technological process. |